CVD金刚石工具膜生长特征SEM观察

本文用不热形变栅状直丝化学气相沉积（ＣＶＤ）法生长金刚石膜，在Ｓｉ及ＷＣ－Ｃｏ硬质合金衬底上金刚石膜晶面显露规律随衬底温度和甲烷浓度而异，经适当表面处理及选择合适的工艺条件，当生长初期衬底上就呈现出良好晶形的沉积膜，衬底与膜之间的粘结力能得到提高。Ｒａｍａｎ谱分析表明此膜仅具有特征金刚石１３３２ｃｍ￣（－１）峰，通过ＳＥＭ观察揭示出盒刚石膜可在表面、侧面及棱上生长，并与衬底有良好的联结。     

无荧光防塌降失水剂KH－931的合成与性能

ＫＨ－９３１是以褐煤、丙烯酰胺、丙烯腈为原料制得的无荧光防塌降失水剂。本文简介了ＫＨ－９３１的合成条件，并对ＫＨ－９３１的防塌作用与降滤失作用进行了室内评定。实验结果表明，ＫＨ－９３１的防塌、降失水效果良好，并具有加量少、无荧光的特点。腐殖酸衍生物，降滤失剂，页岩抑制剂，多功能钻井液处理剂，荧光性，实验室研究     

高分子量聚合物的分子量对岩心渗透率的适应性研究

本文通过不同分子量的高分子量聚合物（部分水解聚丙烯酰胺）在不同渗透率岩心中的流动实验，研究了高分子量聚合物的分子量与岩心渗透率之间的匹配关系，为大庆油田采用高分子量聚合物驱油提供决策依据。     

一维波动方程反演波阻抗的实现及效果

利用波动方程反演波阻抗，由于计算工作量大、稳定性差等原因，一直没有在地震勘探资料处理中得到实际应用。本文提出的一维波方程逐段折叠反演方法能较好地克服上述缺陷，具有计算量相对较小、精度高、稳定性好等特点。并在大庆长垣东部和西部的实际资料处理中见到了良好的效果。     

反偏移法三维波动方程正演

三维地震资料的处理与解释往往都需要三维正演模型给予验证，以得到准确的处理、解释结果。本文提出的三维正演方法是一种偏移算法的逆运算方法－有限差分反偏移法。这一算法具有算法简单、运算量小及深度方向分辨率高的特点，是一种快速、高精度的正演算法。反偏移法虽是偏移算法的逆运算法，却出现常规偏移算法中所没有的很多问题。为此，本文进行了三种不同反偏移方法试验，并采用了一种新的浮动坐标变换，使正演结果精度得到很大     

叠后高分辨率资料处理方法及应用效果

高分辨率勘探是一项系统工程，它由多个环节组成。甚至叠后高发辨率资料处理也是由多个环节组成。本文介绍的叠后高分辨率资料处理流程主要包括Ｌｐ模自适应预测统计反褶积，高频成分补偿，振幅补偿及有色成分校正。文中还就处理流程中各种方法的合理组合，各种方法自身参数的合理选取作了试验和探讨，最后给出了处理实例。     

Micromechanical characterisation of fibre/matrix interfaces

Theoretical analyses for the single fibre pull-out and push-out models under monotonic loading are given which are based on a shear-lag analysis in a fracture mechanics approach considering non-constant friction at the debonded interface as a result of fibre Poisson contraction (or expansion). The solutions allow the determination of typical fibre/matrix interfacial properties such as the interfacial fracture toughness, G_ic, the coefficient of friction, μ, and the residual clamping stress, q₀. Under cyclic loading the interfacial properties are expected to degrade as a result of repetitive abrasion, and a power law function is assumed between μ and the number of elapsed cycles, N. However, G_ic is assumed to be unaffected and a fracture mechanics based debond criterion is derived for the relationship between the external applied stress, the debond length and the reduced friction coefficient for both fibre pull-out and fibre push-out. In addition, the relative displacements between the free fibre end and the matrix top are obtained for cyclic fatigue when the fibre is loaded and unloaded. A relationship obtained for the protrusion (or intrusion) length in fibre pull-out (or push-out) experiments allows the severity of the interface frictional degradation to be evaluated and characterised. Similarities and differences in the frictional degradation behaviour between fibre pull-out and push-out are also identified.     

Microstructure-related fracture toughness and fatigue crack growth behaviour in toughened, anhydride-cured epoxy resins

Fracture toughness and fatigue crack propagation (FCP) of plain and modified anhydride-cured epoxy resin (EP) were studied at ambient temperature. Liquid carboxyl-terminated acrylonitrile-butadiene (CTBN) and silicon (SI) rubber dispersions were used as tougheners for the EP. The morphology of the modified EP was characterized by dynamic mechanical analysis (DMA) and by scanning electron microscopy (SEM). The fracture toughness, K_c, of the compositions decreased with increasing deformation rate. K_c of the EP was slightly improved by CTBN addition and practically unaffected by incorporation of the SI dispersion when tests were performed at low cross-head speed, v. Both modifiers improved K_c at high v, and also the resistance to FCP, by shifting the curves to higher stress intensity factor ranges, ΔK, by comparison with the plain EP. It was established that both fracture and fatigue performance rely on the compliance, J_R, at the rubbery plateau, and thus on the apparent molecular mass between crosslinks, M_c. The failure mechanisms were less dependent upon the loading mode (fracture, fatigue), but differed basically for the various modifiers. Rubber-induced cavitation and shear yielding of the EP were dominant for CTBN, whereas crack bifurcation and branching controlled the cracking in SI-modified EP. The simultaneous use of both modifiers resulted in a synergistic effect for both the fracture toughness at high deformation rate and the FCP behavior.     

PAN共聚纤维的热氧化研究

本工作采用连续式实骏装置与方法,借助力学测试、X射线衍射、元素分析、红外光谱等技术,系统地研究了PAN共聚纤维在连续热氧化过程中化学、结构、性能间的联系,亦对PAN基碳纤维力学性能提高的途径进行了探讨。研究结累表明:在热氧化过程中,PAN共聚体系的热化学反应主要发生在250℃左右;其间纤维的序态结构变化剧烈,易使纤维产生结构缺陷,进而影响热氧化纤维力学性能的变化。     

应用并行技术实现CAD／CAM的高度集成

传统的CAD/CAM系统由于设计思想本身的局限性,其内部只能达到一种松散的基于数据交换的低水平的集成,产品的设计方法也不符合工程技术人员的设计思路。本文提出了基于全耦合的单一数据模型的并行CAD/CAM系统设计思想,使得CAD/CAM系统内部达到以数据共享为基础的高度集成。并行CAD/CAM系统充分体现了工程技术人员的思维方式及产品设计过程的反复性和协调性。此外,文中还提出广义参数化设计的新概念,它与特征设计方法的有机结合保证了产品模型的完整性和产品设计过程的同步性。特征共享是实现CAD和CAM集成的关键因素。并行CAD/CAM系统应用面向对象软件设计思想,实现了复杂数据模型的内部封装,并为数据模型和功能模块之间提供简单直观的界面。面向对象设计方法是开发并行CAD/CAM系统的有效手段。